Welcome to Nanalysis’ benchtop NMR Blog
We love benchtop NMR! In this blog section, you will find all things benchtop NMR. Please contact us if you would like to discuss about your project.
Category
NMR Topics
- 100 MHz NMR
- 11B NMR
- 13C NMR
- 19F NMR
- 19F NMR Spectroscopy
- 31P NMR
- 3H NMR
- Agrochemicals
- Applications
- Batteries
- Biopolymers
- Botanicals
- COSY
- CPMG
- Cannabis
- Chemical Analysis
- Cosmetics
- DEPT
- Dithiazine
- Drug Analysis
- Dyes
- Edible Oils
- Educational NMR
- Energy
- Exchangeable Protons
- Exchangeable protons
- Flavor and Fragrances
- Flow NMR
- Fluorine-19 NMR
- Food Science
- Food and Beverage
- Forensics
- Forestry
- HMBC
- HSQC
- Hands-on Learning
- Hydrogen sulfide
- Hydroxyl value
- Hyphenated NMR
- Illicit Drugs
- Industrial Applications
- Inorganic Chemistry
- Interpretation of NMR
- Interpretation of NMR Spectra
- Inversion-Recovery
- Keto-Enol Tautomerism
- LF vs. HF NMR
- Lignin Analysis
- Literature
- Literature using Nanalysis benchtop NMR
Literature with Benchtop NMR
Are you looking for literature using benchtop NMR? We have compiled a list of reading materials here.
What to expect: Chemical Shifts & Coupling Constants in Low-field NMR Spectroscopy
One of the questions that we always get at tradeshows and conferences is how our instrument compares to high-field data. There are significant inherent differences between low-field and high-field instruments, but the most important from a chemistry point of view are sensitivity (S/N) and resonance dispersion (signal separation). Read More.
Guide: Preparing a Sample for NMR analysis – Part I
In this blog, we highlight the importance choosing the correct NMR solvent and checking the final volume in the NMR tube.
β-Diketone tautomerization ratio determined via 60 MHz benchtop NMR
Tautomers are constitutional isomers that interconvert into each other by an exchange reaction, most commonly a proton transfer. Such two isomers can for example be a ketone and an enol. Read More.
Unsymmetric Carbon Satellites in Fluorine-19 NMR
In the 19F NMR spectrum of DCBTF, we can observe the singlet resonance of the trifluoromethyl fragment at δ = −63.07 ppm. While it might not jump into your eye at first glance, please note that the carbon satellites are not centered at the "main signal", which is what we are used to from 1H NMR spectra. Read more
Beyond Structure Elucidation - Introduction to qNMR Part II - Calibrants
In this blog post, I will talk about how to select a suitable calibrant as well as the difference between using an internal and external calibrant. When conducting qNMR experiments, one of the first things that needs to be considered is how the calibrant is employed to quantitate your sample. Read more.
Carbon-13 Satellites and Molecule Symmetry in Maleic Acid
Symmetry is beauty. There are countless examples in nature, just think about honeycombs, flowers, starfish or….maleic acid! You probably can guess which of these examples will be the star in this blog post - no, sorry, it is not the starfish…
Beyond structural elucidation, introduction to qNMR – Part I
Over the last few years, more and more analytical and industrial laboratories have started employing quantitative nuclear magnetic resonance (qNMR) spectroscopy as a tool for content assignment (due to its superb structural elucidation abilities) and quantification of purity in a sample. Read more.
Unsymmetric Carbon Satellites in Fluorine-19 NMR
In the 19F NMR spectrum of DCBTF, we can observe the singlet resonance of the trifluoromethyl fragment at δ = −63.07 ppm. While it might not jump into your eye at first glance, please note that the carbon satellites are not centered at the "main signal", which is what we are used to from 1H NMR spectra. Read more
Relation between the FID and the NMR spectrum
NMR users can deal with spectrum evaluation in the daily work, but how is the spectrum information stored in the time domain (FID)? Read more.